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photo: Lödige Process Technology
photo: Lödige Process Technology

The manufacture of powder products can sometimes be a big challenge, since small amounts of pigments must be mixed completely evenly with relatively high amounts of carrier substances. Christian Schilken introduces the horizontal ploughshare mixer, which was developed for powder products.

The production of cosmetic powder products requires fast, homogeneous mixing of different components that vary significantly in quantity. With special ploughshare mixers, all the stages of the mixing process can take place in one machine, which means that these mixers represent a very efficient solution to this complex process engineering task. Loose and pressed cosmetic powder products are made up of several ingredients in different ratios. For example, tiny amounts of pigments have to be mixed with large quantities of carrier material. Every stage of the production of these powder products is highly complex. Firstly, the individual components must be mixed quickly and evenly. Next the pigments need to be dissolved without causing streaking. The third step involves adding precise amounts of liquid binding agent and distributing it without flocking to ensure high-quality pressing results. This phase may also include carefully mixing in effect pigments. As a result, highly sensitive and expensive additives, such as mica (CI 77019), have to be processed without causing damage or leading to a deterioration in quality. Another problem is that the temperature of the materials must not exceed a critical level during mixing to ensure that the product does not change colour.

Horizontal mixer

In many cases, the use of horizontal mixers has proved to be the ideal solution to these varied and complex requirements. These mixers operate based on the mechanically generated fluid bed principle developed by Lödige, which ensures a high energy input and produces very good mixing results. In addition, the mixers make it possible for all the stages of the cosmetic powder production process to take place in one machine. This results in short process times and a high level of flexibility. Liquids and other additives can be introduced via a single-substance nozzle in the venting port. The small models in particular, which have a gross volume of 130 or 300 litres, offer the high levels of flexibility needed by manufacturing companies which have small batch sizes and formulations that change frequently. A cooling jacket with a large heat transfer area allows for effective temperature control. The distance between the mixing elements and the wall has been kept to a minimum. By machining the drum, distances of 0.5 to 1.0 mm can be achieved. The result is that only a very small amount of the product remains in the drum after it is emptied, even in the case of highly adhesive materials.

Mixing principle

The central feature of the mixer is a special arrangement of ploughshare shovels on a horizontal shaft. The shovels rotate in a cylindrical mixing vessel, which is positioned horizontally. The size, number, position, shape, and circumferential speed of the shovels are carefully coordinated to create a three-dimensional movement in the materials during the mixing process. This means that the materials are continuously mixed by the mixing tools to prevent dead spots or areas of low movement and to guarantee a quick, precise and reproduceable mixing process. The design of the mixing tools ensures that the mixture is removed from the drum wall in a radial movement to prevent particles becoming stuck between the wall and the mixing tools. The mechanically generated fluid bed principle causes no damage to the product and is ideal for delicate, heat-sensitive substances. Modified shovels can be used depending on the requirements, even for more specific ones. These enables producing the best possible results even when processing the most sensitive products. In some mixing tasks, in particular dissolving pigments and distributing liquid binding  agent, the mixing elements need additional support. For this purpose, serrated choppers can be installed. These have a separate drive system and rotate at high speed. They help with the distribution of substances within the product. The resulting short mixing time together with the efficient use of drive power keeps the energy consumption to a minimum. In addition, a complex two-substance nozzle is not required.

Cosmetic powder products are made up of several ingredients in different ratios. For
Cosmetic powder products are made up of several ingredients in different ratios. For

Hygienic design

Particularly when colour pigments and some other substances are used, it is also essential to prevent the cross-contamination of consecutive batches. The hygienic design of the machine ensures that it can be emptied leaving hardly any residues and, most importantly, can be easily cleaned. This has been made possible by a large inspection door that gives easy access to the entire interior and by the use of ground and polished stainless-steel surfaces. As a general rule, the surface roughness must be smaller than the particle size of the materials that adhere to the surface so that the residue can be directly moistened by the cleaning agents.

Surfaces that come into contact with the product usually have a roughness of Ra < 0.8 μm. The surfaces can be electropolished to further reduce roughness. The mixing elements and choppers have also been specially designed for easy cleaning. The mixing tools and the set of chopper blades are fully welded and have the same surface roughness as the drum wall. Air purge seals or mechanical seals that can be rinsed are generally the best technical solution for use on  mixing tool shafts and choppers. During the production process the shaft seals are purged with compressed air. This prevents the product from penetrating into the gap between the fixed and rotating parts of the seal. The volume flow rate is controlled and assessed via a flow meter and air volume and pressure are displayed on the control panel of the machine control system.

Conclusion

The production of cosmetic powder products involves mixing very small amounts of pigments evenly with the carrier material, dissolving the pigments without causing streaking and distributing the liquid binding agent evenly without flocking to ensure high-quality pressing results. Other requirements include short process times and a high level of flexibility. Horizontal batch mixers with ploughshare shovels and a hygienic design are the ideal solution and allow all the stages of the process to take place in one machine.

Christian Schilken,

Sales Life Science Technology,

Gebr. Lödige Maschinenbau, Paderborn,

Germany,
www.loedige.de 

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